Green’s Dictionary of Slang

rattle and hiss n.

[rhy. sl. = piss n. (2)]

an act of urination.

[US]A.J. Pollock Und. Speaks n.p.: Rattle and hiss, urine.
[US]Maurer & Baker ‘“Aus.” Rhyming Argot’ in AS XIX:3.
[UK]J. Franklyn Dict. Rhy. Sl.
[UK]Dodson & Saczek Dict. of Cockney Rhy. Sl.
[US]Maledicta II:1+2 (Summer/Winter) 117: There are other, more general if less modern and correct, studies of Cockney rhyming slang, though they tend to skirt Tom Tit (‘shit’), rattle [and hiss] (‘piss’), you and me (‘pee’) and me and you (‘screw’).